TY - JOUR
T1 - 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole
AU - Nagaraj, Basavegowda
AU - Narasegowda, Rajenahally S.
AU - Yathirajan, Hemmige S.
AU - Gaonkar, Santhosh L.
AU - Bolte, Michael
PY - 2005/3
Y1 - 2005/3
N2 - The synthesis of 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole, was studied. The 5-(4′-Methylbiphenyl-2-yl)-1H-tetrezole, trityl chloride and triethylamine in dichloromethane were stirred for 2 hours at room temperature. To obtain the compound the recovered product was treated with 1-bromo2,5-pyrrolidinedione and benzoyal peroxide in carbon tetrachloride. It is observed that the compound 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole is recrystallized from ethyl methyl ketone.
AB - The synthesis of 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole, was studied. The 5-(4′-Methylbiphenyl-2-yl)-1H-tetrezole, trityl chloride and triethylamine in dichloromethane were stirred for 2 hours at room temperature. To obtain the compound the recovered product was treated with 1-bromo2,5-pyrrolidinedione and benzoyal peroxide in carbon tetrachloride. It is observed that the compound 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole is recrystallized from ethyl methyl ketone.
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U2 - 10.1107/S1600536805005490
DO - 10.1107/S1600536805005490
M3 - Article
AN - SCOPUS:18544363274
SN - 1600-5368
VL - 61
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
IS - 3
ER -