5-Bromo-3H-isobenzofuran-1-one (5-bromophthalide)

Hemmige S. Yathirajan, Basavegowda Nagaraj, Santhosh L. Gaonkar, Rajenahally S. Narasegowda, Padmarajaiah Nagaraja, Michael Bolte

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

The synthesis and crystal structure of C8H5BrO 2 were investigated. The compound served as a starting materials for the synthesis of citalopram. It crystallized wilth two almost identical molecules in the asymmetric unit. The compound was diazotized with NaNO 2 and concentrated HCl to yield the diazonium salt. The results show that in each molecule, all non-H atoms are coplanar.

Original languageEnglish
JournalActa Crystallographica Section E: Structure Reports Online
Volume61
Issue number2
DOIs
Publication statusPublished - 02-2005

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Citalopram
Molecules
synthesis
molecules
Salts
Crystal structure
salts
Atoms
crystal structure
atoms

All Science Journal Classification (ASJC) codes

  • Chemistry(all)
  • Materials Science(all)
  • Condensed Matter Physics

Cite this

Yathirajan, Hemmige S. ; Nagaraj, Basavegowda ; Gaonkar, Santhosh L. ; Narasegowda, Rajenahally S. ; Nagaraja, Padmarajaiah ; Bolte, Michael. / 5-Bromo-3H-isobenzofuran-1-one (5-bromophthalide). In: Acta Crystallographica Section E: Structure Reports Online. 2005 ; Vol. 61, No. 2.
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5-Bromo-3H-isobenzofuran-1-one (5-bromophthalide). / Yathirajan, Hemmige S.; Nagaraj, Basavegowda; Gaonkar, Santhosh L.; Narasegowda, Rajenahally S.; Nagaraja, Padmarajaiah; Bolte, Michael.

In: Acta Crystallographica Section E: Structure Reports Online, Vol. 61, No. 2, 02.2005.

Research output: Contribution to journalArticle

TY - JOUR

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AU - Yathirajan, Hemmige S.

AU - Nagaraj, Basavegowda

AU - Gaonkar, Santhosh L.

AU - Narasegowda, Rajenahally S.

AU - Nagaraja, Padmarajaiah

AU - Bolte, Michael

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