Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one

G. B. Thippeswamy, D. Vijaykumar, T. N.Mahadeva Prasad, B. S. Jayashree, B. N. Lakshminarayana, M. A. Sridhar, J. Shashidhara Prasad

Research output: Contribution to journalArticle

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Abstract

The compound, 3-(4-ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one, was synthesized by using 4-methoxy-2-hydroxyacetophenone and 4-ethylbenzaldehyde solutions. The synthesized compound was characterized by spectroscopic techniques, and finally confirmed by X-ray diffraction studies. The compound is a dimer in nature, and crystallizes in the triclinic crystal class in the space group P1. The cell parameters are a = 9.6860(9)Å, b = 12.6650(17)Å, c = 13.4990(18)Å,α= 68.808(4),β= 81.149(7), g = 79.863(7), V = 1511.5(3) and Z = 4. In the crystal, O-H·O hydrogen bonds connect the hydroxy donor group and the C=O acceptor group. The R1[I > 2σ(I)] and wR2 (all data) values are 0.0600 and 0.1984, respectively.

Original languageEnglish
Pages (from-to)39-40
Number of pages2
JournalX-ray Structure Analysis Online
Volume27
Issue number7
Publication statusPublished - 07-11-2011

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Crystal symmetry
Dimers
Hydrogen bonds
Crystal structure
X ray diffraction
Crystals
2'-hydroxyacetophenone

All Science Journal Classification (ASJC) codes

  • Analytical Chemistry
  • Materials Chemistry

Cite this

Thippeswamy, G. B., Vijaykumar, D., Prasad, T. N. M., Jayashree, B. S., Lakshminarayana, B. N., Sridhar, M. A., & Prasad, J. S. (2011). Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one. X-ray Structure Analysis Online, 27(7), 39-40.
Thippeswamy, G. B. ; Vijaykumar, D. ; Prasad, T. N.Mahadeva ; Jayashree, B. S. ; Lakshminarayana, B. N. ; Sridhar, M. A. ; Prasad, J. Shashidhara. / Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one. In: X-ray Structure Analysis Online. 2011 ; Vol. 27, No. 7. pp. 39-40.
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abstract = "The compound, 3-(4-ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one, was synthesized by using 4-methoxy-2-hydroxyacetophenone and 4-ethylbenzaldehyde solutions. The synthesized compound was characterized by spectroscopic techniques, and finally confirmed by X-ray diffraction studies. The compound is a dimer in nature, and crystallizes in the triclinic crystal class in the space group P1. The cell parameters are a = 9.6860(9){\AA}, b = 12.6650(17){\AA}, c = 13.4990(18){\AA},α= 68.808(4),β= 81.149(7), g = 79.863(7), V = 1511.5(3) and Z = 4. In the crystal, O-H·O hydrogen bonds connect the hydroxy donor group and the C=O acceptor group. The R1[I > 2σ(I)] and wR2 (all data) values are 0.0600 and 0.1984, respectively.",
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Thippeswamy, GB, Vijaykumar, D, Prasad, TNM, Jayashree, BS, Lakshminarayana, BN, Sridhar, MA & Prasad, JS 2011, 'Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one', X-ray Structure Analysis Online, vol. 27, no. 7, pp. 39-40.

Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one. / Thippeswamy, G. B.; Vijaykumar, D.; Prasad, T. N.Mahadeva; Jayashree, B. S.; Lakshminarayana, B. N.; Sridhar, M. A.; Prasad, J. Shashidhara.

In: X-ray Structure Analysis Online, Vol. 27, No. 7, 07.11.2011, p. 39-40.

Research output: Contribution to journalArticle

TY - JOUR

T1 - Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one

AU - Thippeswamy, G. B.

AU - Vijaykumar, D.

AU - Prasad, T. N.Mahadeva

AU - Jayashree, B. S.

AU - Lakshminarayana, B. N.

AU - Sridhar, M. A.

AU - Prasad, J. Shashidhara

PY - 2011/11/7

Y1 - 2011/11/7

N2 - The compound, 3-(4-ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one, was synthesized by using 4-methoxy-2-hydroxyacetophenone and 4-ethylbenzaldehyde solutions. The synthesized compound was characterized by spectroscopic techniques, and finally confirmed by X-ray diffraction studies. The compound is a dimer in nature, and crystallizes in the triclinic crystal class in the space group P1. The cell parameters are a = 9.6860(9)Å, b = 12.6650(17)Å, c = 13.4990(18)Å,α= 68.808(4),β= 81.149(7), g = 79.863(7), V = 1511.5(3) and Z = 4. In the crystal, O-H·O hydrogen bonds connect the hydroxy donor group and the C=O acceptor group. The R1[I > 2σ(I)] and wR2 (all data) values are 0.0600 and 0.1984, respectively.

AB - The compound, 3-(4-ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one, was synthesized by using 4-methoxy-2-hydroxyacetophenone and 4-ethylbenzaldehyde solutions. The synthesized compound was characterized by spectroscopic techniques, and finally confirmed by X-ray diffraction studies. The compound is a dimer in nature, and crystallizes in the triclinic crystal class in the space group P1. The cell parameters are a = 9.6860(9)Å, b = 12.6650(17)Å, c = 13.4990(18)Å,α= 68.808(4),β= 81.149(7), g = 79.863(7), V = 1511.5(3) and Z = 4. In the crystal, O-H·O hydrogen bonds connect the hydroxy donor group and the C=O acceptor group. The R1[I > 2σ(I)] and wR2 (all data) values are 0.0600 and 0.1984, respectively.

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Thippeswamy GB, Vijaykumar D, Prasad TNM, Jayashree BS, Lakshminarayana BN, Sridhar MA et al. Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one. X-ray Structure Analysis Online. 2011 Nov 7;27(7):39-40.