Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one

G. B. Thippeswamy, D. Vijaykumar, T. N.Mahadeva Prasad, B. S. Jayashree, B. N. Lakshminarayana, M. A. Sridhar, J. Shashidhara Prasad

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Abstract

The compound, 3-(4-ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one, was synthesized by using 4-methoxy-2-hydroxyacetophenone and 4-ethylbenzaldehyde solutions. The synthesized compound was characterized by spectroscopic techniques, and finally confirmed by X-ray diffraction studies. The compound is a dimer in nature, and crystallizes in the triclinic crystal class in the space group P1. The cell parameters are a = 9.6860(9)Å, b = 12.6650(17)Å, c = 13.4990(18)Å,α= 68.808(4),β= 81.149(7), g = 79.863(7), V = 1511.5(3) and Z = 4. In the crystal, O-H·O hydrogen bonds connect the hydroxy donor group and the C=O acceptor group. The R1[I > 2σ(I)] and wR2 (all data) values are 0.0600 and 0.1984, respectively.

Original languageEnglish
Pages (from-to)39-40
Number of pages2
JournalX-ray Structure Analysis Online
Volume27
Issue number7
Publication statusPublished - 07-11-2011

All Science Journal Classification (ASJC) codes

  • Analytical Chemistry
  • Materials Chemistry

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    Thippeswamy, G. B., Vijaykumar, D., Prasad, T. N. M., Jayashree, B. S., Lakshminarayana, B. N., Sridhar, M. A., & Prasad, J. S. (2011). Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one. X-ray Structure Analysis Online, 27(7), 39-40.