Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime

T. N. Mahadeva Prasad, S. L. Gaonkar, Kamini Kapoor, Vivek K. Gupta, H. Shimizu, M. A. Sridhar, J. Shashidhara Prasad

Research output: Contribution to journalComment/debate

1 Citation (Scopus)

Abstract

The title compound, C 15H 17N 3O 2, was synthesized, and the structure was characterised spectroscopically by 1H NMR and 13C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group Pī with the following cell parameters: a = 7.3332(8)Å, b = 8.6358(7)Å, c = 11.7675Å, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11)Å 3. 2012

Original languageEnglish
Pages (from-to)25-26
Number of pages2
JournalX-ray Structure Analysis Online
Volume28
Issue number4
Publication statusPublished - 2012

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Crystal structure
Nuclear magnetic resonance
Crystal symmetry
X ray diffraction

All Science Journal Classification (ASJC) codes

  • Analytical Chemistry
  • Materials Chemistry

Cite this

Mahadeva Prasad, T. N., Gaonkar, S. L., Kapoor, K., Gupta, V. K., Shimizu, H., Sridhar, M. A., & Shashidhara Prasad, J. (2012). Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime. X-ray Structure Analysis Online, 28(4), 25-26.
Mahadeva Prasad, T. N. ; Gaonkar, S. L. ; Kapoor, Kamini ; Gupta, Vivek K. ; Shimizu, H. ; Sridhar, M. A. ; Shashidhara Prasad, J. / Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime. In: X-ray Structure Analysis Online. 2012 ; Vol. 28, No. 4. pp. 25-26.
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title = "Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime",
abstract = "The title compound, C 15H 17N 3O 2, was synthesized, and the structure was characterised spectroscopically by 1H NMR and 13C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group Pī with the following cell parameters: a = 7.3332(8){\AA}, b = 8.6358(7){\AA}, c = 11.7675{\AA}, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11){\AA} 3. 2012",
author = "{Mahadeva Prasad}, {T. N.} and Gaonkar, {S. L.} and Kamini Kapoor and Gupta, {Vivek K.} and H. Shimizu and Sridhar, {M. A.} and {Shashidhara Prasad}, J.",
year = "2012",
language = "English",
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pages = "25--26",
journal = "X-ray Structure Analysis Online",
issn = "1883-3578",
publisher = "Japan Society for Analytical Chemistry",
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}

Mahadeva Prasad, TN, Gaonkar, SL, Kapoor, K, Gupta, VK, Shimizu, H, Sridhar, MA & Shashidhara Prasad, J 2012, 'Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime', X-ray Structure Analysis Online, vol. 28, no. 4, pp. 25-26.

Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime. / Mahadeva Prasad, T. N.; Gaonkar, S. L.; Kapoor, Kamini; Gupta, Vivek K.; Shimizu, H.; Sridhar, M. A.; Shashidhara Prasad, J.

In: X-ray Structure Analysis Online, Vol. 28, No. 4, 2012, p. 25-26.

Research output: Contribution to journalComment/debate

TY - JOUR

T1 - Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime

AU - Mahadeva Prasad, T. N.

AU - Gaonkar, S. L.

AU - Kapoor, Kamini

AU - Gupta, Vivek K.

AU - Shimizu, H.

AU - Sridhar, M. A.

AU - Shashidhara Prasad, J.

PY - 2012

Y1 - 2012

N2 - The title compound, C 15H 17N 3O 2, was synthesized, and the structure was characterised spectroscopically by 1H NMR and 13C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group Pī with the following cell parameters: a = 7.3332(8)Å, b = 8.6358(7)Å, c = 11.7675Å, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11)Å 3. 2012

AB - The title compound, C 15H 17N 3O 2, was synthesized, and the structure was characterised spectroscopically by 1H NMR and 13C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group Pī with the following cell parameters: a = 7.3332(8)Å, b = 8.6358(7)Å, c = 11.7675Å, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11)Å 3. 2012

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M3 - Comment/debate

VL - 28

SP - 25

EP - 26

JO - X-ray Structure Analysis Online

JF - X-ray Structure Analysis Online

SN - 1883-3578

IS - 4

ER -

Mahadeva Prasad TN, Gaonkar SL, Kapoor K, Gupta VK, Shimizu H, Sridhar MA et al. Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime. X-ray Structure Analysis Online. 2012;28(4):25-26.