Synthesis and Crystal Structure Studies of Novel 4-Tosyloxychalcone Derivative

Shubhalaxmi; B. Geidner; C. S.C. Kumar; H. K. Fun; K. S. Bhat

doi:10.1080/15421406.2015.1036502

Synthesis and Crystal Structure Studies of Novel 4-Tosyloxychalcone Derivative

Shubhalaxmi, B. Geidner, C. S.C. Kumar, H. K. Fun, K. S. Bhat

Research output: Contribution to journal › Article › peer-review

7 Citations (Scopus)

Abstract

4-Tosyloxychalcone derivative, C23H20O4S, was synthesized and characterized by infrared and ¹H NMR spectral studies. Grown crystal was further characterized by single crystal X-ray diffraction studies. The compound crystallizes in monoclinic space group C2/c with unit cell parameters a = 33.431 (6) Å, b = 5.8451 (10) Å, c = 21.439 (4) Å, Z = 8, and V = 3848.2 (12) Å³. The crystal packing is mainly stabilized by C - H.π interaction. There are no significant intermolecular interactions beyond van der Waals forces observed in the solid state structure of the compound.

Original language	English
Pages (from-to)	365-371
Number of pages	7
Journal	Molecular Crystals and Liquid Crystals
Volume	623
Issue number	1
DOIs	https://doi.org/10.1080/15421406.2015.1036502
Publication status	Published - 12-12-2015

All Science Journal Classification (ASJC) codes

Chemistry(all)
Materials Science(all)
Condensed Matter Physics

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title = "Synthesis and Crystal Structure Studies of Novel 4-Tosyloxychalcone Derivative",

abstract = "4-Tosyloxychalcone derivative, C23H20O4S, was synthesized and characterized by infrared and 1H NMR spectral studies. Grown crystal was further characterized by single crystal X-ray diffraction studies. The compound crystallizes in monoclinic space group C2/c with unit cell parameters a = 33.431 (6) {\AA}, b = 5.8451 (10) {\AA}, c = 21.439 (4) {\AA}, Z = 8, and V = 3848.2 (12) {\AA}3. The crystal packing is mainly stabilized by C - H.π interaction. There are no significant intermolecular interactions beyond van der Waals forces observed in the solid state structure of the compound.",

author = "Shubhalaxmi and B. Geidner and Kumar, {C. S.C.} and Fun, {H. K.} and Bhat, {K. S.}",

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T1 - Synthesis and Crystal Structure Studies of Novel 4-Tosyloxychalcone Derivative

AU - Shubhalaxmi,

AU - Geidner, B.

AU - Kumar, C. S.C.

AU - Fun, H. K.

AU - Bhat, K. S.

PY - 2015/12/12

Y1 - 2015/12/12

N2 - 4-Tosyloxychalcone derivative, C23H20O4S, was synthesized and characterized by infrared and 1H NMR spectral studies. Grown crystal was further characterized by single crystal X-ray diffraction studies. The compound crystallizes in monoclinic space group C2/c with unit cell parameters a = 33.431 (6) Å, b = 5.8451 (10) Å, c = 21.439 (4) Å, Z = 8, and V = 3848.2 (12) Å3. The crystal packing is mainly stabilized by C - H.π interaction. There are no significant intermolecular interactions beyond van der Waals forces observed in the solid state structure of the compound.

AB - 4-Tosyloxychalcone derivative, C23H20O4S, was synthesized and characterized by infrared and 1H NMR spectral studies. Grown crystal was further characterized by single crystal X-ray diffraction studies. The compound crystallizes in monoclinic space group C2/c with unit cell parameters a = 33.431 (6) Å, b = 5.8451 (10) Å, c = 21.439 (4) Å, Z = 8, and V = 3848.2 (12) Å3. The crystal packing is mainly stabilized by C - H.π interaction. There are no significant intermolecular interactions beyond van der Waals forces observed in the solid state structure of the compound.

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JO - Molecular Crystals and Liquid Crystals

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Synthesis and Crystal Structure Studies of Novel 4-Tosyloxychalcone Derivative

Abstract

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