Synthesis and Crystal Structure Studies of Novel 4-Tosyloxychalcone Derivative

Shubhalaxmi, B. Geidner, C. S.C. Kumar, H. K. Fun, K. S. Bhat

Research output: Contribution to journalArticle

6 Citations (Scopus)

Abstract

4-Tosyloxychalcone derivative, C23H20O4S, was synthesized and characterized by infrared and 1H NMR spectral studies. Grown crystal was further characterized by single crystal X-ray diffraction studies. The compound crystallizes in monoclinic space group C2/c with unit cell parameters a = 33.431 (6) Å, b = 5.8451 (10) Å, c = 21.439 (4) Å, Z = 8, and V = 3848.2 (12) Å3. The crystal packing is mainly stabilized by C - H.π interaction. There are no significant intermolecular interactions beyond van der Waals forces observed in the solid state structure of the compound.

Original languageEnglish
Pages (from-to)365-371
Number of pages7
JournalMolecular Crystals and Liquid Crystals
Volume623
Issue number1
DOIs
Publication statusPublished - 12-12-2015

Fingerprint

Crystal structure
Derivatives
Van der Waals forces
Crystals
crystal structure
synthesis
crystals
Nuclear magnetic resonance
Single crystals
interactions
Infrared radiation
solid state
X ray diffraction
nuclear magnetic resonance
single crystals
cells
diffraction
x rays

All Science Journal Classification (ASJC) codes

  • Chemistry(all)
  • Materials Science(all)
  • Condensed Matter Physics

Cite this

Shubhalaxmi ; Geidner, B. ; Kumar, C. S.C. ; Fun, H. K. ; Bhat, K. S. / Synthesis and Crystal Structure Studies of Novel 4-Tosyloxychalcone Derivative. In: Molecular Crystals and Liquid Crystals. 2015 ; Vol. 623, No. 1. pp. 365-371.
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Synthesis and Crystal Structure Studies of Novel 4-Tosyloxychalcone Derivative. / Shubhalaxmi; Geidner, B.; Kumar, C. S.C.; Fun, H. K.; Bhat, K. S.

In: Molecular Crystals and Liquid Crystals, Vol. 623, No. 1, 12.12.2015, p. 365-371.

Research output: Contribution to journalArticle

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AU - Kumar, C. S.C.

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AB - 4-Tosyloxychalcone derivative, C23H20O4S, was synthesized and characterized by infrared and 1H NMR spectral studies. Grown crystal was further characterized by single crystal X-ray diffraction studies. The compound crystallizes in monoclinic space group C2/c with unit cell parameters a = 33.431 (6) Å, b = 5.8451 (10) Å, c = 21.439 (4) Å, Z = 8, and V = 3848.2 (12) Å3. The crystal packing is mainly stabilized by C - H.π interaction. There are no significant intermolecular interactions beyond van der Waals forces observed in the solid state structure of the compound.

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